Metallization of nanosized objects


Conducting and semi-conducting nanoparticles are currently a topic of intense research due to their novel properties, which are significantly different from those of the corresponding bulk materials. Since the unique properties of these nanoparticles are directly related to their size, a precise control over the size, size polydispersity, shape and internal structure is required. As a typical example, the band gap of a semi-conductor nanoparticle is reported to depend on particle size.
Five arm star-shaped block copolymers with a poly(ethylene oxide) (PEO) core and a poly(ε-caprolactone) (PCL) corona were used as templates for the preparation of gold and palladium nanoparticles of improved stability against aggregation. The PEO core of these star-shaped block copolymers could be swollen with KAuCl
4 or Pd(OAc)2 in N,N-dimethylformamide (DMF) and Au or Pd nanoparticles were respectively obtained by reduction. The resulting well defined Au or Pd nanoparticles were stabilized against aggregation thanks to a barrier of PCL chains. Transmission electron microscopy (TEM) experiments strongly suggested that one Au or Pd nanoparticle was formed inside each star-shaped block copolymer. The stability of the accordingly prepared nanoparticles over aggregation was however strongly dependent on the length of the PCL chains.

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Schematic representation of the five-arm PEO-b-PCL copolymer used as template for the synthesis of Au or Pd nanoparticles. A typical TEM picture of gold nanoparticles templated in this copolymer is also shown.


The Pd nanoparticles were evaluated for their capability to act as catalysts in Heck catalyzed coupling reactions utilizing automated synthesizer techniques in combination with GC-MS high-throughput screening. High activities and up to 99% conversion were observed for the coupling of styrene with 4-bromoacetophenone within 24 hours at a catalyst loading of 0.1 mol %.

Researchers involved: Mariam Filali

Collaborations: Ulrich Schubert (Eindhoven), Michael Meier (Eindhoven)

Relevant papers:

"Star-block copolymers as templates for the preparation of stable gold nanoparticles"
M. Filali, M. A. R. Meier, Ulrich S. Schubert, J.-F. Gohy
Langmuir 2005, 21, 7995-8000

"Star-shaped block copolymer stabilized palladium nanoparticles for efficient catalytic Heck cross-coupling reactions"
M. A. R. Meier, M. Filali, J.-F. Gohy, U. S. Schubert
J. Mater. Chem. 2006, 16, 3001-3006

"Star-shaped block copolymers stabilized Pd-nanoparticles and their catalytic activity: a high-throughput approach"
M.A. R. Meier, M. Filali, J.-F. Gohy, U. S. Schubert
Polymer Preprints 2006, 47, 931-932