NMR Complements

lchm2152  2021-2022  Louvain-la-Neuve

NMR Complements
3.00 credits
22.5 h + 7.5 h
Q1
Teacher(s)
Singleton Michael;
Language
English
Main themes
1. Principles and calculations of NMR spectra;
2. 1D NMR pulse sequences (SEFT, APT, INEPT, DEPT);
3. 2D NMR :
a) through bond homonuclear (COSY) and heteronuclear correlations;
b) through space correlations (NOE, NOESY, ROESY);
4. 1H & 13C NMR spectroscopy;
5. NMR spectroscopy of other nuclei (19F, 15N, 31P);
6. Solid state NMR spectroscopy.
Learning outcomes

At the end of this learning unit, the student is able to :

1 This course aims at enlarging and deepening the basic notions in NMR so that students should be able to collect and interpret spectra of various complexities.
 
Content
1. Introduction and generalities;
2. NMR spectroscopy practical aspects;
3. 1D NMR experiments;
4. 2D NMR experiments: through bond homonuclear and heteronuclear correlations, and through space correlations;
5. Solid state NMR;
6. Theoretical aspects and applications will be connected with practical questions related to the use of a NMR spectrometer and data acquisition.
Other information
Background :
Basic notions in molecular spectroscopy (CHM1251B).
Evaluation: written and oral exams.
Documents: complicated schemes (syllabus) may be given along with some textbook references;
The course could be partly or totally delivered by an invited lecturer. Other
Teaching materials
  • matériel sur moodle
Faculty or entity
CHIM


Programmes / formations proposant cette unité d'enseignement (UE)

Title of the programme
Sigle
Credits
Prerequisites
Learning outcomes
Master [120] in Chemistry

Master [60] in Chemistry