Note from June 29, 2020
Although we do not yet know how long the social distancing related to the Covid-19 pandemic will last, and regardless of the changes that had to be made in the evaluation of the June 2020 session in relation to what is provided for in this learning unit description, new learnig unit evaluation methods may still be adopted by the teachers; details of these methods have been - or will be - communicated to the students by the teachers, as soon as possible.
Although we do not yet know how long the social distancing related to the Covid-19 pandemic will last, and regardless of the changes that had to be made in the evaluation of the June 2020 session in relation to what is provided for in this learning unit description, new learnig unit evaluation methods may still be adopted by the teachers; details of these methods have been - or will be - communicated to the students by the teachers, as soon as possible.
3 credits
30.0 h
Q1
Teacher(s)
Fustin Charles-André; Garcia Yann;
Language
French
Aims
At the end of this learning unit, the student is able to : | |
| 1 | This course not only aims at giving a large introduction to the main instrumental analysis methods of solids but also aims at directing an analysis towards the most appropriate solutions. The emphasis is shed on principles, application ranges, possibilities and limitations of each technique. |
The contribution of this Teaching Unit to the development and command of the skills and learning outcomes of the programme(s) can be accessed at the end of this sheet, in the section entitled “Programmes/courses offering this Teaching Unit”.
Content
Content I. Thermal analysis methods: thermogravimetric analysis (TGA), thermodifferential analysis (TDA), differential scanning calorimetry (DSC) II. Surface techniques analysis methods and microscopies: X-ray photoelectrons spectroscopy (XPS), Auger electron spectroscopy (AES). Secondary ions mass spectrometry (SIMS). Specific surface measurement (BET). Scanning electronic microscopy (SEM). Transmission electronic microscopy (TEM). Atomic force microscopy (AFM), Scanning tunneling microscopy (STM) III. X-Ray diffraction and X-ray fluorescence IV. X-Ray absorption spectroscopy : EXAFS, XANES and WAXS V. Mössbauer spectroscopy
Teaching methods
Classes and potential visit of experimental facilities
Evaluation methods
oral exam or written exam depending on the number of registered students
Other information
Background: Molecular symmetry and crystal structures (CHM 1251A) - Fundamentals of molecular spectroscopy (CHM 1251B). The course could be partly or totally delivered by an invited lecturer.
Online resources
Moodle
Bibliography
Instrumental Methods of Analysis, H.H. Willard, L.L. Merritt Jr. J.A. Dean, F. A. Settle Jr., 7th ed., New York, Wadsworth Publishing Company, 1988.
A booklet containing a copy of the overhead transparencies used by the teachers.
Other books that are chapter specific are advised below:
Most of the chapters:
Principles of Instrumental Analysis – 6th Ed., D.A. Skoog, F.J. Holler, S.R. Crouch,Thomson, Books/Cole, 2007
Thermal analysis methods:
DSC, An Introduction for practitionners, G. Höhne, W. Hemminger, H.-J. Flammershein, Springer Verlag, 1996, MOST A1 library : n° 714
Introduction to Instrumental Analysis, R. D. Braun, Mc Graw-Hill, Int. Ed. 1987, Singapore, ISBN 0-07-100147-6, MOST A1 library : n° 669
Materials characterization : Introduction to microscopic and spectroscopic methods, Yang Leng, Wiley, 2008, Réf : A187077 (BST)
X-ray absorption, diffraction and fluorescence
EXAFS : Basic Principles and Data Analysis, K.T. Boon, Springer Verlag, 1986, MOST A1 library : n° 713
Nuclear instruments and their uses – Vol. I : Ionization, detectors, scintillators, Ed. A.H. Snell, John Wiley & Sons, New York, 1962
Principles and practice of X-ray spectrometric analysis, E. P. Bertin, Plenum Press, New York, 1975.
Mössbauer Spectroscopy
Mössbauer spectroscopy and Transition Metal Chemistry, Fundamentals and Applications, P. Gütlich, E. Bill, A. X. Trautwein, Springer, 2011, Ref : A 1 15 QC462.T86 .G (BST), also available in MOST A1 library.
Mössbauer spectroscopy, N. N. Greenwood, T. C. Gibb, London : Chapman and Hall, 1971, Ref : B602672 (BST)
Mössbauer effects in lattice dynamics : experimental, technique and applications, Yi-Long Chen, Wiley VCH, 2007, Ref : A115025 (BST)
Mössbauer spectroscopy, Tutorials for BAC3 level, Y. Yoshida, G. Langouche Eds., Springer, 2013, Ref. A 1 14 QC491.M (BST), also available in MOST A1 library.
A booklet containing a copy of the overhead transparencies used by the teachers.
Other books that are chapter specific are advised below:
Most of the chapters:
Principles of Instrumental Analysis – 6th Ed., D.A. Skoog, F.J. Holler, S.R. Crouch,Thomson, Books/Cole, 2007
Thermal analysis methods:
DSC, An Introduction for practitionners, G. Höhne, W. Hemminger, H.-J. Flammershein, Springer Verlag, 1996, MOST A1 library : n° 714
Introduction to Instrumental Analysis, R. D. Braun, Mc Graw-Hill, Int. Ed. 1987, Singapore, ISBN 0-07-100147-6, MOST A1 library : n° 669
Materials characterization : Introduction to microscopic and spectroscopic methods, Yang Leng, Wiley, 2008, Réf : A187077 (BST)
X-ray absorption, diffraction and fluorescence
EXAFS : Basic Principles and Data Analysis, K.T. Boon, Springer Verlag, 1986, MOST A1 library : n° 713
Nuclear instruments and their uses – Vol. I : Ionization, detectors, scintillators, Ed. A.H. Snell, John Wiley & Sons, New York, 1962
Principles and practice of X-ray spectrometric analysis, E. P. Bertin, Plenum Press, New York, 1975.
Mössbauer Spectroscopy
Mössbauer spectroscopy and Transition Metal Chemistry, Fundamentals and Applications, P. Gütlich, E. Bill, A. X. Trautwein, Springer, 2011, Ref : A 1 15 QC462.T86 .G (BST), also available in MOST A1 library.
Mössbauer spectroscopy, N. N. Greenwood, T. C. Gibb, London : Chapman and Hall, 1971, Ref : B602672 (BST)
Mössbauer effects in lattice dynamics : experimental, technique and applications, Yi-Long Chen, Wiley VCH, 2007, Ref : A115025 (BST)
Mössbauer spectroscopy, Tutorials for BAC3 level, Y. Yoshida, G. Langouche Eds., Springer, 2013, Ref. A 1 14 QC491.M (BST), also available in MOST A1 library.
Teaching materials
- syllabus LCHM2122 Méthodes physiques d'analyse des solides (à la DUC)
Faculty or entity
CHIM
