NMR Complements

lchm2152  2019-2020  Louvain-la-Neuve

NMR Complements
Note from June 29, 2020
Although we do not yet know how long the social distancing related to the Covid-19 pandemic will last, and regardless of the changes that had to be made in the evaluation of the June 2020 session in relation to what is provided for in this learning unit description, new learnig unit evaluation methods may still be adopted by the teachers; details of these methods have been - or will be - communicated to the students by the teachers, as soon as possible.
3 credits
22.5 h + 7.5 h
Q1
Teacher(s)
Luhmer Michel;
Language
English
Main themes
1. Principles and calculations of NMR spectra; 2. 1D NMR pulse sequences (SEFT, APT, INEPT, DEPT); 3. 2D NMR: a) through bond homonuclear (COSY) and heteronuclear correlations; b) through space correlations (NOE, NOESY, ROESY); 4. 1H & 13C NMR spectroscopy; 5. NMR spectroscopy of other nuclei (19F, 15N, 31P); 6. Solid state NMR spectroscopy.
Aims

At the end of this learning unit, the student is able to :

1 This course aims at enlarging and deepening the basic notions in NMR so that students should be able to collect and interpret spectra of various complexities.
 

The contribution of this Teaching Unit to the development and command of the skills and learning outcomes of the programme(s) can be accessed at the end of this sheet, in the section entitled “Programmes/courses offering this Teaching Unit”.
Content
1. Introduction and generalities; 2. NMR spectroscopy practical aspects; 3. 1D NMR experiments; 4. 2D NMR experiments: through bond homonuclear and heteronuclear correlations, and through space correlations; 5. Solid state NMR; 6. Theoretical aspects and applications will be connected with practical questions related to the use of a NMR spectrometer and data acquisition.
Other information
Background: Basic notions in molecular spectroscopy (CHM1251B). Evaluation: written and oral exams. Documents: complicated schemes (syllabus) may be given along with some textbook references; The course could be partly or totally delivered by an invited lecturer. Other
Teaching materials
  • matériel sur moodle
Faculty or entity
CHIM


Programmes / formations proposant cette unité d'enseignement (UE)

Title of the programme
Sigle
Credits
Prerequisites
Aims
Master [60] in Chemistry

Master [120] in Chemistry