22.5 h + 7.5 h
1. Principles and calculations of NMR spectra; 2. 1D NMR pulse sequences (SEFT, APT, INEPT, DEPT); 3. 2D NMR: a) through bond homonuclear (COSY) and heteronuclear correlations; b) through space correlations (NOE, NOESY, ROESY); 4. 1H & 13C NMR spectroscopy; 5. NMR spectroscopy of other nuclei (19F, 15N, 31P); 6. Solid state NMR spectroscopy.
At the end of this learning unit, the student is able to :
|1||This course aims at enlarging and deepening the basic notions in NMR so that students should be able to collect and interpret spectra of various complexities.|
The contribution of this Teaching Unit to the development and command of the skills and learning outcomes of the programme(s) can be accessed at the end of this sheet, in the section entitled “Programmes/courses offering this Teaching Unit”.
1. Introduction and generalities; 2. NMR spectroscopy practical aspects; 3. 1D NMR experiments; 4. 2D NMR experiments: through bond homonuclear and heteronuclear correlations, and through space correlations; 5. Solid state NMR; 6. Theoretical aspects and applications will be connected with practical questions related to the use of a NMR spectrometer and data acquisition.
Background: Basic notions in molecular spectroscopy (CHM1251B). Evaluation: written and oral exams. Documents: complicated schemes (syllabus) may be given along with some textbook references; The course could be partly or totally delivered by an invited lecturer. Other
Faculty or entity