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Organic analysis I : separation techniques [ LBIR1318 ]


6.0 crédits ECTS  60.0 h + 30.0 h   2q 

Teacher(s) Jerkovic Vesna ; Collin Sonia (coordinator) ;
Language French
Place
of the course
Louvain-la-Neuve
Online resources

Icampus

Prerequisites

Organic chemistry  CHIM1170

Main themes

- Properties of chemical compounds

- Strategy of an organic analysis

- Methods for extraction and concentration

- Gas chromatography

- High-pressure liquid chromatography

- Modification of the properties by derivatisation

- Methods of quantification

- Semi-preparative HPLC

- UPLC

- Enantiomeric separations

 

Aims

a. Contribution de l'activité au référentiel AA (AA du programme)

The course contributes to the following learning outcomes : 1, 3 and 6 (BIR program)

b. Formulation spécifique pour cette activité des AA du programme (maximum 10)

At the end of this course, the student will be able to select the best technique to get rid of all major co-constituents, to optimize the resolution of the GC/HPLC chromatograms, to choose the best detector in terms of sensibility and selectivity, to accurately quantify the analytes (use of internal standards, external standards, standard addition, isotopic dilution ..) and to extrapolate the concepts to isolate them by (semi)preparative HPLC or GC.

Evaluation methods

Written examination for the theoretical part. 3 Oral communications (in English) are presented during the seminars (discussion of experimental protocols). The experimental know-how and the attitude are evaluated throughout practical classes (laboratory report).

Teaching methods

Half of the courses consist in magistral lectures, the other part being a reflection (groups of students) around published experimental protocols. The students have also the opportunity to apply a few number of experimental protocols at the laboratory.

Content

- Properties of chemical compounds

- Strategy of an organic analysis

- Methods for extraction and concentration

- Gas chromatography

- High-pressure liquid chromatography

- Modification of the properties by derivatisation

- Methods of quantification

- Semi-preparative HPLC

- UPLC

- Enantiomeric separations

Bibliography

No particular support which would be paying are required.

Cycle et année
d'étude
> Bachelor in Bioengineering
Faculty or entity
in charge
> AGRO


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